Handbook of analysis of oligonucleotides and related products (Boca Raton, 2011). - ОГЛАВЛЕНИЕ / CONTENTS
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ОбложкаHandbook of analysis of oligonucleotides and related products / ed. by J.V.Bonilla, G.S.Srivatsa. - Boca Raton: CRC, 2011. - xiv, 497 p. - Incl. bibl. ref. - Ind.: p.487-497. - ISBN 978-1-4398-1993-7
 

Оглавление / Contents
 
Preface ......................................................... v
Editors ....................................................... vii
Contributors ................................................... ix
Introduction ................................................... xi

Chapter 1  Purity Analysis and Impurities Determination by
           Reversed-Phase High-Performance Liquid
           Chromatography ....................................... 1
           Hagen Cramer, Kevin J. Finn, and Eric Herzberg
Chapter 2  Purity Analysis and Impurities Determination by
           AEX-HPLC ............................................ 47
           Jim Thayer, Veeravagu Murugaiah, and Yansheng Wu
Chapter 3  Purity Analysis and Molecular Weight 
           Determination by Size Exclusion HPLC ............... 105
           Ming Fai Chan and Ipsita Roymoulik
Chapter 4  Analysis of Oligonucleotides by Liquid
           Chromatography and Mass Spectrometry ............... 137
           Soheil Pourshahian and Sean M. McCarthy
Chapter 5  Sequence Determination and Confirmation by MS/MS
           and MALDI-TOF ...................................... 167
           Zoltan Timar
Chapter 6  Tm Analysis of Oligonucleotides .................... 219
           Huihe Zhu and G. Susan Srivatsa
Chapter 7  Purity and Content Analysis of Oligonucleotides
           by Capillary Gel Electrophoresis ................... 243
           Judy Carmody and Bernhard Noll
Chapter 8  Bioanalysis of Therapeutic Oligonucleotides
           Using Hybridization-Based Immunoassay
           Techniques ......................................... 265
           Helen Legakis and Sandra Carriero
Chapter 9  Oligonucleotide Assay and Potency .................. 285
           Dennis P. Michaud
Chapter 10 Microbial Analysis: Endotoxin Testing .............. 307
           Barbara J. Markley
Chapter 11 Analysis of Residual Solvents by Head Space Gas
           Chromatography ..................................... 331
           Sky Countryman and Jose V. Bonilla
Chapter 12 Determination of Extinction Coefficient ............ 351
           Veeravagu Murugaiah
Chapter 13 Structural Determination by NMR .................... 361
           Michele L. DeRider, Doug Brooks, and Gary Burt
Chapter 14 Infrared Analysis of Oligonucleotides .............. 385
           Jose V. Bonilla
Chapter 15 Stability Indicating Methods for Oligonucleotide
           Products ........................................... 403
           Veeravagu Murugaiah
Chapter 16 Analysis by Hydrophilic Interaction
           Chromatography ..................................... 425
           Renee N. Easter and Patrick A. Limbach
Chapter 17 Determination of Base Composition .................. 439
           Hüseyin Aygün
Chapter 18 Analysis of Metals in Oligonucleotides ............. 453
           Michael P. Murphy
Chapter 19 Regulatory Considerations for the Development of
           Oligonucleotide Therapeutics ....................... 465
           G. Susan Srivatsa

Index ......................................................... 487


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